Carbon Dioxide → HCID 20289059, compound

HRID 1413958Notes

Reaction equation

HRID 1413958 reaction equation
[CH2:1]([OH:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13]CCCCC.[CH2:20]([C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[OH:33])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].[O-2].[Ba+2:35].[C:36](=[O:38])=[O:37]>O>[C:36](=[O:19])([O-:38])[O-:37].[Ba+2:35].[CH2:20]([C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[O-:33])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].[Ba+2:35].[CH2:7]([C:6]1[CH:5]=[CH:4][CH:3]=[CH:2][C:1]=1[O-:19])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Participants

6

Reactant 4

HCID 280Carbon DioxideHCID 336682-HeptylphenolHCID 5284499Oleyl AlcoholHCID 9855530Barium Oxide Nanoparticle Dispersion

Product 1

HCID 20289059HCID 20289059, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To a mixture of 268 grams (1.0 equivalent) oleyl alcohol, 124 grams (0.6 equivalent) of heptylphenol, 1000 grams of mineral oil, and 190 grams of water was added at 70° C. 306 grams (4.0 equivalents) of barium oxide. This mixture was heated at reflux temperature for an hour and then treated with carbon dioxide at 150° C. until the mixture was neutral. The mixture was filtered through Hyflo to yield a liquid product having the following analyses:

Workup

  1. additionwas added at 70° C
  2. temperatureThis mixture was heated
  3. temperatureat reflux temperature for an hour
  4. filtrationThe mixture was filtered through Hyflo
  5. customto yield a liquid product

Sources & evidence

ORD record
ord-8ebbab44bf1447cebbd29f8493f5771e
Source dataset
uspto-grants-1981_02
Patent number
US04252698

Reaction notes

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