HRID1413958

反应详情

EQUATION

反应方程式

HRID 1413958 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a mixture of 268 grams (1.0 equivalent) oleyl alcohol, 124 grams (0.6 equivalent) of heptylphenol, 1000 grams of mineral oil, and 190 grams of water was added at 70° C. 306 grams (4.0 equivalents) of barium oxide. This mixture was heated at reflux temperature for an hour and then treated with carbon dioxide at 150° C. until the mixture was neutral. The mixture was filtered through Hyflo to yield a liquid product having the following analyses:

WORKUP

后处理

  1. additionwas added at 70° C
  2. temperatureThis mixture was heated
  3. temperatureat reflux temperature for an hour
  4. filtrationThe mixture was filtered through Hyflo
  5. customto yield a liquid product