HRID1413958
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a mixture of 268 grams (1.0 equivalent) oleyl alcohol, 124 grams (0.6 equivalent) of heptylphenol, 1000 grams of mineral oil, and 190 grams of water was added at 70° C. 306 grams (4.0 equivalents) of barium oxide. This mixture was heated at reflux temperature for an hour and then treated with carbon dioxide at 150° C. until the mixture was neutral. The mixture was filtered through Hyflo to yield a liquid product having the following analyses:
WORKUP
后处理
- additionwas added at 70° C
- temperatureThis mixture was heated
- temperatureat reflux temperature for an hour
- filtrationThe mixture was filtered through Hyflo
- customto yield a liquid product