HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 54233991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 12791329 | HCID 12791329 | — |
| Product | HCID 54233991 | HCID 54233991 | 84% |
Reaction Steps
28.9 g (0.2 mol) of 3-methoxy-3-methyl-2,4-dioxa-bicyclo[3,2,0]heptane (stereoisomer mixture) and 15.4 g (0.2 mol) of acetyl chloride are heated to the reflux for 5 hours. Distillation in vacuo gives 24.8 g (84%) of trans-1-chloro-2-acetoxy-cyclobutane. Boiling point19 79°, nD20 1.4473.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04252738 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-ed7052004e0d4ac1b0a7803039312e93 |
| Source note | uspto-grants-1981_02 |