HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Morpholinecarbonyl chloride → 4-Morpholinecarboxylic acid, 3,4,5-trimethoxyphenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Morpholinecarbonyl chloride | HCID 84810 | — |
| Reactant | HCID 23684108 | HCID 23684108 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-Morpholinecarboxylic acid, 3,4,5-trimethoxyphenyl ester | HCID 3051877 | — |
Reaction Steps
To a solution of 10.15 g (0.049 mole) sodium 3,4,5-trimethoxyphenolate in 100 ml anhydrous dimethylformamide are added gradually, with stirring, 7.5 g (0.050 mole) N-chloroformyl-morpholine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04252804 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-d85994d77e7943158d246cdec90a3226 |
| Source note | uspto-grants-1981_02 |