HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 54176741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 21447337 | HCID 21447337 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54176741 | HCID 54176741 | — |
Reaction Steps
1.06 ml of 100% nitric acid are slowly added dropwise at -10° to a solution of 5.9 g of 4-cyclohexyl-2-hydroxy-phenylacetic acid in 100 ml of absolute methylene chloride. The mixture is finally stirred for 10 minutes without further cooling, the methylene chloride solution washed several times with water, dried over sodium sulphate and evaporated to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04252817 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-0718a6c7756b4a7e9a03faafa529caac |
| Source note | uspto-grants-1981_02 |