HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lactic Acid → 2-(Dimethylamino)ethyl 2-hydroxypropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lactic Acid | HCID 612 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 2-(Dimethylamino)ethanol | HCID 7902 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-(Dimethylamino)ethyl 2-hydroxypropanoate | HCID 14179203 | — |
Reaction Steps
The resin of this example was prepared in the presence of 5 percent water based on total solids, and had a water-to-amine nitrogen (of the amine acid salt) equivalency of 1.74:0.44. A dimethyl ethanolamine lactate was prepared by admixing 13.3 parts of dimethyl ethanolamine and 18.0 parts of lactic acid (85 percent solution in water). The mixture was held at 40°C. to 60°C. for a short time and there was then added 7.2 parts of isopropanol. The final composition consisted of 75 percent solids and contained 7.1 percent water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001156 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-db4ef79f13dd4ffdb27569ee3dae6cbc |
| Source note | uspto-grants-1977_01 |