HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediamine → 1,3-Propanediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediamine | HCID 428 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | 1,3-Propanediamine | HCID 428 | — |
| Product | Azetidine | HCID 10422 | — |
Reaction Steps
A catalyst as described in Example 2 is charged to the reactor and its temperature raised to 150°C under a flow of hydrogen. When a feed of 1,3-diamino propane is passed over the catalyst at LHSV 0.4 at mole ratio H2 :H2N(CH2)3NH2 of 15 a conversion of the feed of 10% at high selectivity to azetidine results.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001213 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-8765c41acba74ba1b971b875e6ba4db3 |
| Source note | uspto-grants-1977_01 |