HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetate-hydrochloric acid → HCID 70632897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetate-hydrochloric acid | HCID 22641269 | — |
| Reactant | HCID 70633446 | HCID 70633446 | — |
| Product | HCID 70632897 | HCID 70632897 | — |
Reaction Steps
The 3-(t-butoxycarbonyl-aminopropionyl)-1-{[5-(4-fluorophenyl) furfurylidene]amino}hydantoin (10.4 g, 0.023 mole) was added to 3% HCl/acetic acid (125 ml) and stirred for 4 hours. The yellow solid was filtered, washed with nitromethane and ether to yield 7 g, 28%, m.p. 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001222 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-a887c4e7cb5646fc985d3c5bff4dbcf1 |
| Source note | uspto-grants-1977_01 |