Benzoic acid, 4-amino-3-nitro- → HCID 21486319, compound

HRID 1414184Notes

Reaction equation

HRID 1414184 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[NH2:13])[C:7]([OH:9])=[O:8])([O-:3])=[O:2].[CH:14]1([C:17](Cl)=[O:18])[CH2:16][CH2:15]1>>[CH:14]1([C:17]([NH:13][C:12]2[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][C:4]=2[N+:1]([O-:3])=[O:2])=[O:18])[CH2:16][CH2:15]1

Participants

3

Reactant 2

HCID 74115Benzoic acid, 4-amino-3-nitro-HCID 77637Cyclopropanecarbonyl chloride

Product 1

HCID 21486319HCID 21486319, compound

Procedure

The acylation of 7.0 g (0.0384 mol) of 3-nitro-4-amino-benzoic acid with 4.42 g (0.0423 mol) of cyclopropanecarboxylic acid chloride was carried out as described in Example 3.

Sources & evidence

ORD record
ord-035ccc8babe64a8e9c9c2796fb40964b
Source dataset
uspto-grants-1977_01
Patent number
US04001218

Reaction notes

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