1-Iodopropane → HCID 21486852, compound

Participants

Reaction Steps

The title compound was prepared from ethyl 1,3,4-oxadiazole-2-thione-5-carboxylate potassium salt dimethylsulfoxide solvate (10 g., 28.5 mmole) and n-propyliodide (4.17 ml., 42.8 mmole) analogously to the procedure described in Experiment A. The yield was 4.99 g. (81%). The product had a B.P. of 108°-118° C. at 0.65 mm. of mercury.

Provenance & Evidence