HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → Boron trifluoride etherate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Boron trifluoride etherate | HCID 8000 | — |
| Product | Dimethyl Ether | HCID 8254 | — |
Reaction Steps
Another method for the alkylation of the 3-hydroxy is by reaction with an alcohol in the presence of boron trifluoride etherate. Thus, methanol and boron trifluoride etherate yield a methyl ether at a reaction temperature of about 25° C. followed conveniently by thin layer chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001300 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-34ecc80fd69f4fb3b1962b1e33176e4d |
| Source note | uspto-grants-1977_01 |