HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromide ion → HCID 21507434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromide ion | HCID 259 | — |
| Reactant | 3-Chloro-2-methyl-1-propene | HCID 11241 | — |
| Reactant | Desmethylclobazam | HCID 89657 | — |
| Product | HCID 21507434 | HCID 21507434 | — |
Reaction Steps
In the same manner by acting (2'-methylallyl) chloride or bromide in the presence of a metallation agent, starting from 1-phenyl 8-chloro 1,2,4,5-tetrahydro 2,4-dioxo 3H-1,5-benzodiazepine, there is obtained 1-phenyl 5-(2'-methylallyl) 8-chloro 1,2,4,5-tetrahydro 2,4-dioxo 3H-1,5-benzodiazepine (R1 = H, R2 = Cl R3 = ##STR20## R4 = C6H5) melting at 149°-151° C upon recrystallisation in 50 % ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001408 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-c75661b6ef5b4b1481b6fa8617a4f6cc |
| Source note | uspto-grants-1977_01 |