HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21487992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Diethylaminoethyl chloride | HCID 13364 | — |
| Reactant | HCID 21487920 | HCID 21487920 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21487992 | HCID 21487992 | — |
Reaction Steps
2-p-Hydroxyphenyl-3-(3',5'-dimethylbenzoyl)benzofuran (5.25 g., 15.3 mmol.) was dissolved in 200 ml. of dry acetone and 10.5 g. (0.076 mol.) of potassium carbonate and 2.10 g. (15.3 mmol.) of 2-diethylaminoethyl chloride were added. The reaction mixture was refluxed for three hours, then it was cooled and filtered. The filtrate was concentrated at reduced pressure to give the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001426 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-f3021689b5424ac09203357e407fc367 |
| Source note | uspto-grants-1977_01 |