HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → HCID 21487980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(1-Benzofuran-2-yl)phenol | HCID 10125163 | — |
| Solvent | Ethyl ketone | HCID 7288 | — |
| Product | HCID 21487980 | HCID 21487980 | — |
Reaction Steps
A mixture of 10.5 g. (0.05 mol.) of 2-p-hydroxyphenylbenzofuran and 47 g. (0.25 mol.) of 1,2-dibromoethane in 200 ml. of 3-pentanone containing 46 g. (0.3 mol.) of potassium carbonate was heated at 100° for 12 hours. The mixture was filtered while hot and the solid remaining was washed with hot acetone. The combined filtrate and washings were concentrated to give 2-[4'-(2-bromoethoxy)phenyl]benzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001426 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-533545304e0a46c2a6fe7388c120d843 |
| Source note | uspto-grants-1977_01 |