Diethylamine → HCID 21488035, compound

HRID 1414616Notes

Reaction equation

Br[CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2[O:12][C:13]3[CH:31]=[CH:30][CH:29]=[CH:28][C:14]=3[C:15]=2[C:16](=[O:27])[C:17]2[CH:22]=[C:21]([CH3:23])[C:20]([O:24][CH3:25])=[C:19]([CH3:26])[CH:18]=2)=[CH:7][CH:6]=1.[CH2:32]([NH:34][CH2:35][CH3:36])[CH3:33]>>[CH2:32]([N:34]([CH2:35][CH3:36])[CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2[O:12][C:13]3[CH:31]=[CH:30][CH:29]=[CH:28][C:14]=3[C:15]=2[C:16](=[O:27])[C:17]2[CH:22]=[C:21]([CH3:23])[C:20]([O:24][CH3:25])=[C:19]([CH3:26])[CH:18]=2)=[CH:7][CH:6]=1)[CH3:33]

Participants

Reactant 2

HCID 8021Diethylamine

HCID 21487933HCID 21487933, compound

Product 1

HCID 21488035HCID 21488035, compound

Procedure

Reaction of 2-[4'-(2-bromoethoxy)phenyl]-3-(3',5'-dimethyl-4-methoxybenzoyl)benzofuran with diethylamine as described in Example 11 gave the title compound.

Sources & evidence

ORD record: ord-92c32435806448fd9fefd1c6b05094be
Source dataset: uspto-grants-1977_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04001426

Reaction notes

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