HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4-[(Methoxymethyl)sulfanyl]-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-{4-[(Methoxymethyl)sulfanyl]-2-nitrophenyl}acetamide | HCID 20362834 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-[(Methoxymethyl)sulfanyl]-2-nitroaniline | HCID 20362817 | — |
Reaction Steps
1.4 G. of 1 -acetamido-2-nitro-4-methoxymethylthiobenzene is treated in 6 ml. of methanol with 3 ml. of 5N aqueous sodium hydroxide solution and refluxed for 15 minutes. The solvent is removed under vacuum and the residue diluted with water and extracted with chloroform. Evaporation of the chloroform yields 2-nitro-4-methoxymethylthioaniline as reddish crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002640 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-c9e10d95db21402f8b26ad4a8167a651 |
| Source note | uspto-grants-1977_01 |