HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 2-nitro-N-2-propenyl- → HCID 12000044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 2-nitro-N-2-propenyl- | HCID 10888479 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12000044 | HCID 12000044 | — |
Reaction Steps
35 g of 2-nitro-N-allylaniline in 400 ml of methanol are hydrogenated in the presence of 1.5 g of the catalyst described in Example 6, at 75° C and 100-120 bars of hydrogen, for 1.5 hours, to give N-allyl-o-phenylenediamine. The solution which has been freed from the catalyst by filtration is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002673 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-4dbe217d94af4210bd4fc76dad8be692 |
| Source note | uspto-grants-1977_01 |