HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[4-(2-pyridyl)butylamino]ethylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | 4-(Pyridin-2-yl)butan-1-amine | HCID 13511083 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-Nitro-2-methylthio-2-[4-(2-pyridyl)butylamino]ethylene | HCID 70619237 | — |
Reaction Steps
2-(4-Aminobutyl)pyridine was reacted with 1-nitro-2,2-bis-methylthio-ethylene in pyridine at 60° for 3.5 hours. Concentration of the reaction mixture and crystallisation yielded 1-nitro-2-methylthio-2-[4-(2-pyridyl)butylamino]ethylene, m.p. 78°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002759 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-ddcfdb851440463b886b2378596f3841 |
| Source note | uspto-grants-1977_01 |