HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 1-Nitro-2-methylamino-2-[4-(2-pyridyl)butylamino]ethylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1-Nitro-2-methylthio-2-[4-(2-pyridyl)butylamino]ethylene | HCID 70619237 | — |
| Product | 1-Nitro-2-methylamino-2-[4-(2-pyridyl)butylamino]ethylene | HCID 70619517 | — |
Reaction Steps
A mixture of 1-nitro-2-methylthio-2-[4-(2-pyridyl)-butylamino]ethylene and 33% ethanolic methylamine were heated on a steam bath for 15 minutes. Concentration, followed by crystallisation from ethyl acetate yielded the title compound m.p. 90°-91°. (Found: C, 57.8; H, 7.2; N, 22.6%. C12H18N4O2 requires: C, 57.6; H, 7.2; N, 22.4 %).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002759 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-7c76eea86c1f46f99296299377c73bc8 |
| Source note | uspto-grants-1977_01 |