Acetic Anhydride → HCID 21485402, compound

HRID 1415072Notes

Reaction equation

HRID 1415072 reaction equation
[CH2:1]([O:3][CH:4]([O:8][CH2:9][CH3:10])[CH2:5][CH2:6][NH2:7])[CH3:2].[C:11](OC(=O)C)(=[O:13])[CH3:12]>N1C=CC=CC=1>[CH2:1]([O:3][CH:4]([O:8][CH2:9][CH3:10])[CH2:5][CH2:6][NH:7][C:11](=[O:13])[CH3:12])[CH3:2]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 5210291-Amino-3,3-diethoxypropane

Product 1

HCID 21485402HCID 21485402, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

In similar manner, treat 3-aminopropanal diethylacetal with acetic anhydride in pyridine, then treat resulting 3-acetamidopropanal diethylacetal with acid to obtain 3-acetamidopropanal.

Workup

  1. additiontreat

Sources & evidence

ORD record
ord-80b6f1026fb343bc8427e37f6efce68c
Source dataset
uspto-grants-1977_01
Patent number
US04002742

Reaction notes

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