HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 20390077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Reactant | HCID 14449820 | HCID 14449820 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20390077 | HCID 20390077 | — |
Reaction Steps
5.1 gms. of [[(phenylthio)methyl]thio]acetic acid, potassium salt are treated with 5 gms. of oxalyl chloride in 10 ml. of methylene chloride at 0°-5° to obtain 3.4 gms. of [[(phenylthio)methyl]thio]acetyl chloride which is used further without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04003893 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-9199a3f3ab7d43b7bd3b9a65a8c61146 |
| Source note | uspto-grants-1977_01 |