Oxalyl chloride → HCID 20390077, compound

HRID 1415115Notes

Reaction equation

HRID 1415115 reaction equation
[C:1]1([S:7][CH2:8][S:9][CH2:10][C:11]([OH:13])=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[K].C(Cl)(=O)C([Cl:18])=O>C(Cl)Cl>[C:1]1([S:7][CH2:8][S:9][CH2:10][C:11]([Cl:18])=[O:13])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

5

Reactant 3

HCID 65578Oxalyl chlorideHCID 5462222PotassiumHCID 14449820HCID 14449820, compound

Product 1

HCID 20390077HCID 20390077, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

5.1 gms. of [[(phenylthio)methyl]thio]acetic acid, potassium salt are treated with 5 gms. of oxalyl chloride in 10 ml. of methylene chloride at 0°-5° to obtain 3.4 gms. of [[(phenylthio)methyl]thio]acetyl chloride which is used further without purification.

Workup

  1. customof [[(phenylthio)methyl]thio]acetyl chloride which is used further without purification

Sources & evidence

ORD record
ord-9199a3f3ab7d43b7bd3b9a65a8c61146
Source dataset
uspto-grants-1977_01
Patent number
US04003893

Reaction notes

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