Lithium Hydroxide → HCID 23718939, compound

HRID 1415169Notes

Reaction equation

HRID 1415169 reaction equation
[F:1][C:2]1[CH:7]=[C:6]([F:8])[CH:5]=[CH:4][C:3]=1[NH:9][C:10]([C:12]1[CH2:17][CH2:16][CH2:15][CH2:14][C:13]=1[C:18]([O-:20])=[O:19])=[O:11].C[NH+](C)C.[OH-].[Li+:26]>>[F:1][C:2]1[CH:7]=[C:6]([F:8])[CH:5]=[CH:4][C:3]=1[NH:9][C:10]([C:12]1[CH2:17][CH2:16][CH2:15][CH2:14][C:13]=1[C:18]([O-:20])=[O:19])=[O:11].[Li+:26]

Participants

3

Reactant 2

HCID 3939Lithium HydroxideHCID 21483883HCID 21483883, compound

Product 1

HCID 23718939HCID 23718939, compound

Procedure

Six parts of trimethylammonium 2-(2,4-difluorophenylaminocarbonyl)-1-cyclohexene-1-carboxylate were dissolved in 10 parts of 2N lithium hydroxide solution. The solution was evaporated under reduced pressure of 20 mm Hg. at 50° C to 4.5 parts of lithium 2-(2,4-difluorophenylaminocarbonyl)-1-cyclohexene-1-carboxylate as a white solid melting 210°-225° C.

Workup

  1. customThe solution was evaporated under reduced pressure of 20 mm Hg
  2. customat 50° C
  3. custommelting 210°-225° C.

Sources & evidence

ORD record
ord-7563e7732f7041e18d86552251be469d
Source dataset
uspto-grants-1977_01
Patent number
US04003926

Reaction notes

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