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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1415171Generated: October 26, 2026

Oxalate → N-(2-dimethylamino-ethyl)-5H-dibenzo[a,d]cyclohepten-5-imine oxalate

https://huagongshe.com/reaction/1415171

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalateHCID 71081—
Reactant3-Chloro-5H-dibenzo[A,D][7]annulen-5-oneHCID 12690610—
Reactant3-chloro-N-(2-dimethylamino-ethyl)-5H-dibenzo[a,d]cyclohepten-5-imineHCID 21483807—
ReactantN,N-DimethylaminoethylamineHCID 57041336—
ProductN-(2-dimethylamino-ethyl)-5H-dibenzo[a,d]cyclohepten-5-imine oxalateHCID 21483813—

Reaction Steps

from 3-chloro-5H-dibenzo[a,d]cyclohepten-5-one and N,N-dimethylamino-ethylamine, there is obained 3-chloro-N-(2-dimethylamino-ethyl)-5H-dibenzo[a,d]cyclohepten-5-imine, melting point 173°-175° C. (oxalate);

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04003915
Source datasetuspto-grants-1977_01
ORD IDord-87c90f6567e74ca2b970e35b871f20d2
Source noteuspto-grants-1977_01