HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86734423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | HCID 21411013 | HCID 21411013 | — |
| Reactant | HCID 21411018 | HCID 21411018 | — |
| Product | HCID 86734423 | HCID 86734423 | — |
Reaction Steps
Using the procedure described in Example IV but substituting an equivalent amount of N-{-2-[0-chloro-α-(p-fluorophenyl)benzyloxy]ethyl}acetamide for the N-{2-[bis(p-fluorophenyl)methoxy]ethyl}acetamide and maleic acid for the hydrogen chloride, there is obtained 2-[ 0 -chloro-α-(p-fluorophenyl)benzyloxy]ethylamine hydrogen maleate, which is crystallised from ethanol. Its melting point is 123°-123.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04003932 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-6a9881b8386d4d3b9ad38d55d912f134 |
| Source note | uspto-grants-1977_01 |