HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21483905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Chloroacetonitrile | HCID 7856 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 21483899 | HCID 21483899 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21483905 | HCID 21483905 | — |
Reaction Steps
A stirred mixture of 2-cyclopentyl-6-hydroxy-7,8-dichloro-1-tetralone (2.9 g., 0.1 mole), potassium carbonate (15.2 g., 0.11 mole) and chloroacetonitrile (7.5 g., 0.10 mole) in DMF (100 ml.) is heated at 55°-60° C. for two hours and poured into water. The 2-cyclopentyl-6-cyanomethoxy-7,8-dichloro-1-tetralone that separates is collected and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04003927 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-79847d5f036d495a89281729f831d7bf |
| Source note | uspto-grants-1977_01 |