HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Nitro-4-(3-phenylpropoxy)benzene → Aniline, p-(3-phenylpropoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Nitro-4-(3-phenylpropoxy)benzene | HCID 21481845 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | Aniline, p-(3-phenylpropoxy)- | HCID 42154 | — |
Reaction Steps
99 g of 4-(3'-phenyl-propoxy)-nitrobenzene is dissolved in 2000 ml of methanol and hydrogenated with Raney nickel until the absorption of hydrogen is completed. The catalyst is filtered off and the filtrate is concentrated by evaporation to obtain, as a crystalline residue, 4-(3'-phenylpropoxy)-aniline having a melting point of 55°- 57°. -
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04004907 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-b76eb5365a4e442faeb86e2e4339cc8a |
| Source note | uspto-grants-1977_01 |