HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15739784, compound → HCID 15717143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15739784 | HCID 15739784 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15717143 | HCID 15717143 | — |
Reaction Steps
86 g of 4-(2'-phenyl-ethylthio)-nitrobenzene is dissolved in 900 ml of methanol and catalytically hydrogenated with Raney nickel. After completion of the absorption of hydrogen, the catalyst is filtered off and the filtrate is concentrated by evaporation. There is obtained 4-(2'-phenyl-ethylthio)-aniline as oily residue, which is used without purification in the next reaction stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04004907 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-d10bfe646bd847acad87b0650e9d2499 |
| Source note | uspto-grants-1977_01 |