HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 57125898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | HCID 3362042 | HCID 3362042 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | HCID 57125898 | HCID 57125898 | — |
Reaction Steps
The procedure of Example IX using 32.1 g of 1-cyclopropyl-3-(p-methylphenyl)prop-2-en-1-one, 16.5 ml of nitroethane and 2.1 g of sodium in 170 ml of methanol gives 32 g of 1-cyclopropyl-3-(p-methylphenyl)-4-nitropentanone which is used in the crude state for the remainder of the operations.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04005103 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-080357f21aad40c69124858081bdcc75 |
| Source note | uspto-grants-1977_01 |