Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trimethylamine | HCID 1146 | — |
| Reactant | N-Methylbenzylamine | HCID 7669 | — |
| Reactant | HCID 21481846 | HCID 21481846 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 70632541 | HCID 70632541 | — |
Reaction Steps
To 0.25 moles of bromomethylmethyldimethoxysilane is added 0.25 moles of methylbenzylamine, and the mixture is heated to 100° C. for 12 hours. At the end of that time, 300 ml of hexane is added and excess trimethylamine is added. This mixture is allowed to stir for 3 hours, filtered, and the hexane is removed under reduced pressure, leaving benzylmethylaminomethylmethyldimethoxysilane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04005118 |
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| Source dataset | uspto-grants-1977_01 |
|---|
| ORD ID | ord-521d2d6b9e16418fa22849a04c213d75 |
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| Source note | uspto-grants-1977_01 |
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