Trimethylamine → HCID 70632541, compound

HRID 1415444Notes

Reaction equation

HRID 1415444 reaction equation
Br[CH2:2][Si:3]([CH3:8])([O:6][CH3:7])[O:4][CH3:5].CN[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[CH3:18][N:19](C)C>CCCCCC>[CH2:11]([CH2:18][NH:19][CH2:2][Si:3]([CH3:8])([O:6][CH3:7])[O:4][CH3:5])[C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

Participants

5

Reactant 3

HCID 1146TrimethylamineHCID 7669N-MethylbenzylamineHCID 21481846HCID 21481846, compound

Product 1

HCID 70632541HCID 70632541, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Conditions

Temperature
100 °C

Procedure

To 0.25 moles of bromomethylmethyldimethoxysilane is added 0.25 moles of methylbenzylamine, and the mixture is heated to 100° C. for 12 hours. At the end of that time, 300 ml of hexane is added and excess trimethylamine is added. This mixture is allowed to stir for 3 hours, filtered, and the hexane is removed under reduced pressure, leaving benzylmethylaminomethylmethyldimethoxysilane.

Workup

  1. filtrationfiltered
  2. customthe hexane is removed under reduced pressure

Sources & evidence

ORD record
ord-521d2d6b9e16418fa22849a04c213d75
Source dataset
uspto-grants-1977_01
Patent number
US04005118

Reaction notes

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