Dimethylcarbamoyl Chloride → HCID 4396936, compound

HRID 1415474Notes

Reaction equation

[CH2:1]([N:3]([CH2:17]C)[C:4]([NH:6][CH:7]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH2:10][CH2:9][CH2:8]1)=[O:5])C.CN(C)C(Cl)=O>>[CH3:1][N:3]([CH3:17])[C:4]([NH:6][CH:7]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH2:10][CH2:9][CH2:8]1)=[O:5]

Participants

Reactant 2

HCID 6598Dimethylcarbamoyl Chloride

HCID 21393488HCID 21393488, compound

Product 1

HCID 4396936HCID 4396936, compound

Procedure

1,1-Diethyl-3-(1,2,3,4-tetrahydro-1-naphthyl)urea, melting point 86° C. to 87° C., is prepared by the above procedure, by substituting diethylcarbamyl chloride for dimethylcarbamyl chloride.

Sources & evidence

ORD record: ord-7f56f35ccd474caaa40792607b192770
Source dataset: uspto-grants-1977_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04005140

Reaction notes

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