HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 52055-23-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 5-(Benzyloxy)tryptamine | HCID 89576 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 52055-23-9 | HCID 2828785 | — |
Reaction Steps
An ethyl acetate solution saturated with hydrochloric acid was added to a solution of 10 g of 5-benzyloxy-tryptamine in 200 ml of isopropanol until the pH was 1-2 and the mixture was vacuum filtered. The crystals were washed with ethyl acetate and dried under reduced pressure to obtain 11.3 g of 5-benzyloxy-tryptamine hydrochloride melting at 250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04005206 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-1c1a01720dc44e5eb030897af143d39e |
| Source note | uspto-grants-1977_01 |