Ethyl Acrylate → HCID 20386809, compound

HRID 1415553Notes

Reaction equation

HRID 1415553 reaction equation
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=[CH2:3].[CH:8]1([NH2:11])[CH2:10][CH2:9]1>>[CH:8]1([N:11]([CH2:3][CH2:2][C:1]([O:5][CH2:6][CH3:7])=[O:4])[CH2:3][CH2:2][C:1]([O:5][CH2:6][CH3:7])=[O:4])[CH2:10][CH2:9]1

Participants

3

Reactant 2

HCID 8821Ethyl AcrylateHCID 69828Cyclopropylamine

Product 1

HCID 20386809HCID 20386809, compound

Procedure

A mixture of 400 g. of ethyl acrylate (containing 0.75% hydroquinone inhibitor) and 114 g. of cyclopropylamine is heated in a bomb in an oil bath at 175° C. for 10 hours. The reaction mixture is then removed and distilled in vacuo to give N-cyclopropyl-N,N-di(β-carbethoxyethyl)amine.

Workup

  1. additionA mixture of 400 g
  2. customThe reaction mixture is then removed
  3. distillationdistilled in vacuo

Sources & evidence

ORD record
ord-a3410b10873f435691c6e19204a02173
Source dataset
uspto-grants-1977_01
Patent number
US04005208

Reaction notes

Loading…