HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Diethoxy-1-(phenylmethyl)piperidine → HCID 21482822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Diethoxy-1-(phenylmethyl)piperidine | HCID 21482878 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 21482822 | HCID 21482822 | — |
Reaction Steps
A mixture of 15 g. of 1-benzyl-3,3-diethoxypiperidine in 100 ml. of absolute alcohol and 0.5 g. of 10% palladium on charcoal is shaken over 50 p.s.i. of hydrogen at 50° C. for six hours. The catalyst is filtered and washed with ethanol. The solvent is removed by distillation to give 3,3-diethoxypiperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04005208 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-c68437865866452186479d43a9b44b81 |
| Source note | uspto-grants-1977_01 |