Glycolide → HCID 131720991, compound

HRID 1415704Notes

Reaction equation

[CH2:1]1[O:8]C(=O)C[O:4][C:2]1=[O:3].[C:9]1(=[O:16])[O:15][CH2:14][CH2:13][O:12][C:10]1=[O:11]>>[C:2]([OH:4])(=[O:3])[CH2:1][OH:8].[C:9]1(=[O:16])[O:15][CH2:14][CH2:13][O:12][C:10]1=[O:11]

Participants

Reactant 2

HCID 65432Glycolide

HCID 137967Ethylene oxalate

Product 1

HCID 131720991HCID 131720991, compound

Procedure

Polymerization and post-treatment were performed in the same manner as in Polymer Preparation Example 1 except that a mixture of 210 g of glycolide and 10 g of ethylene oxalate (1,4-dioxane-2,3-dione) was used in place of 220 g of glycolide, thereby obtaining a glycolic acid-ethylene oxalate copolymer [Polymer (P-2)]. The same process was conducted repeatedly to prepare a necessary amount of Polymer (P-2).

Workup

customPolymerization

Sources & evidence

ORD record: ord-19ad3679c44a4b9e887e494af26e648a
Source dataset: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05908917

Reaction notes

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