Trimethylsilyl cyanide → HCID 21862840, compound

HRID 1415744Notes

Reaction equation

HRID 1415744 reaction equation
[F:1][C:2]1[CH:19]=[CH:18][C:5]([N:6]=[CH:7][C:8]2[CH:13]=[CH:12][C:11]([S:14](=[O:17])(=[O:16])[NH2:15])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.C[Si]([C:24]#[N:25])(C)C>>[F:1][C:2]1[CH:19]=[CH:18][C:5]([NH:6][CH:7]([C:8]2[CH:13]=[CH:12][C:11]([S:14](=[O:17])(=[O:16])[NH2:15])=[CH:10][CH:9]=2)[C:24]#[N:25])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 82115Trimethylsilyl cyanideHCID 21862753HCID 21862753, compound

Product 1

HCID 21862840HCID 21862840, compound

Procedure

Following a procedure similar to that described in Example 1(ii), but using 4-fluoro-N-(4-sulfamoylbenzylidene)aniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a slightly yellow powder (yield 83%).

Sources & evidence

ORD record
ord-f317704dc2a445c8a1597b1b51031bc4
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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