Trimethylsilyl cyanide → HCID 21862817, compound

HRID 1415753Notes

Reaction equation

HRID 1415753 reaction equation
[CH3:1][C:2]1[CH:17]=[CH:16][C:5]([CH:6]=[N:7][C:8]2[CH:13]=[CH:12][C:11]([S:14][CH3:15])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.C[Si]([C:22]#[N:23])(C)C>>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([CH:6]([NH:7][C:8]2[CH:13]=[CH:12][C:11]([S:14][CH3:15])=[CH:10][CH:9]=2)[C:22]#[N:23])=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 82115Trimethylsilyl cyanideHCID 21862770HCID 21862770, compound

Product 1

HCID 21862817HCID 21862817, compound

Procedure

Following a procedure similar to that described in Example 1(ii), but using N-(4-methylbenzylidene)-4-methylthioaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a pale yellow powder (yield 73%).

Sources & evidence

ORD record
ord-aaaa31d1c7d241cb93d4f5dd6ecc8e64
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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