p-Toluidine → N-(4-Sulfamoylbenzylidene)-4-methylaniline

HRID 1415776Notes

Reaction equation

[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2].[CH3:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][CH:15]=1>>[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=[N:18][C:17]2[CH:19]=[CH:20][C:14]([CH3:13])=[CH:15][CH:16]=2)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2]

Participants

Reactant 2

HCID 7813p-Toluidine

HCID 1510884-Sulfamoylbenzaldehyde

Product 1

HCID 21862824N-(4-Sulfamoylbenzylidene)-4-methylaniline

Procedure

Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-methylaniline as starting materials, the title compound was obtained as a yellow powder (yield 82%).

Sources & evidence

ORD record: ord-ccc50503d20a417d92b2494d77b95924
Source dataset: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05908858

Reaction notes

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