Trimethylsilyl cyanide → HCID 21862819, compound

HRID 1415780Notes

Reaction equation

HRID 1415780 reaction equation
[Cl:1][C:2]1[CH:19]=[CH:18][C:5]([N:6]=[CH:7][C:8]2[CH:13]=[CH:12][C:11]([S:14](=[O:17])(=[O:16])[NH2:15])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.C[Si]([C:24]#[N:25])(C)C>>[Cl:1][C:2]1[CH:19]=[CH:18][C:5]([NH:6][CH:7]([C:8]2[CH:13]=[CH:12][C:11]([S:14](=[O:17])(=[O:16])[NH2:15])=[CH:10][CH:9]=2)[C:24]#[N:25])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 82115Trimethylsilyl cyanideHCID 21862848HCID 21862848, compound

Product 1

HCID 21862819HCID 21862819, compound

Procedure

Following a procedure similar to that described in Example 1(ii), but using 4-chloro-N-(4-sulfamoylbenzylidene)aniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a white powder (yield 93%).

Sources & evidence

ORD record
ord-6f870d938ce84051a6693ccba08cdee0
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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