HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53960015, compound → HCID 53780169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53960015 | HCID 53960015 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 53780169 | HCID 53780169 | 41.7% |
Reaction Steps
This compound was prepared following the procedure of Synthetic Example 1(n), using the product (54.4 g) from step (e). Chromatography on silica gel, using hexane:EtOAc (9:1) as eluant, gave the title product (22.8 g) as an orange oil. 1H NMR consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05910494 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-65ad03af4caf4c90819cccd823eaa3e7 |
| Source note | uspto-grants-1999_06 |