Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 53763934 | HCID 53763934 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 53796098 | HCID 53796098 | 69.9% |
Reaction Steps
To 8 ml of acetic acid and 10 ml of 6N hydrochloric acid was added 1.3 g of the compound synthesized in Example 235. The solution was stirred at 100° C. for 4 hours. The solvent was distilled off in vacua. Water was added to the residue. The solid was collected by filtration and washed with water, ethanol, and isopropyl ether to give 0.55 g of the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05910498 |
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| Source dataset | uspto-grants-1999_06 |
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| ORD ID | ord-a925b4fca5024d60bfac470ea4c978c0 |
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| Source note | uspto-grants-1999_06 |
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