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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1415969Generated: October 31, 2026

Hydrochloric Acid → HCID 53796098, compound

https://huagongshe.com/reaction/1415969

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 53763934HCID 53763934—
SolventAcetic AcidHCID 176—
ProductHCID 53796098HCID 5379609869.9%

Reaction Conditions

Temperature100 °C

Reaction Steps

To 8 ml of acetic acid and 10 ml of 6N hydrochloric acid was added 1.3 g of the compound synthesized in Example 235. The solution was stirred at 100° C. for 4 hours. The solvent was distilled off in vacua. Water was added to the residue. The solid was collected by filtration and washed with water, ethanol, and isopropyl ether to give 0.55 g of the title compound as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05910498
Source datasetuspto-grants-1999_06
ORD IDord-a925b4fca5024d60bfac470ea4c978c0
Source noteuspto-grants-1999_06