HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoamylamine → HCID 178446282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoamylamine | HCID 7894 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178418667 | HCID 178418667 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178446282 | HCID 178446282 | — |
Reaction Steps
2-Amino-4-chloro-6-hydroxy-5-nitropyrimidine (4 g), 3-methylbutylamine (1.8 g) and triethylamine (6 ml) were heated at reflux for 5 h then left stirring overnight at room temperature in ethanol. The precipitate was filtered and washed with water and air dried to yield the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05912252 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-05df86ae2c654bfb99b5cb8b89a3d49b |
| Source note | uspto-grants-1999_06 |