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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1416165Generated: November 3, 2026

Isoamylamine → HCID 178446282, compound

https://huagongshe.com/reaction/1416165

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsoamylamineHCID 7894—
ReactantTriethylamineHCID 8471—
ReactantHCID 178418667HCID 178418667—
SolventEthanolHCID 702—
ProductHCID 178446282HCID 178446282—

Reaction Steps

2-Amino-4-chloro-6-hydroxy-5-nitropyrimidine (4 g), 3-methylbutylamine (1.8 g) and triethylamine (6 ml) were heated at reflux for 5 h then left stirring overnight at room temperature in ethanol. The precipitate was filtered and washed with water and air dried to yield the title compound as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05912252
Source datasetuspto-grants-1999_06
ORD IDord-05df86ae2c654bfb99b5cb8b89a3d49b
Source noteuspto-grants-1999_06