Hydrochloric Acid → HCID 70200256, compound

HRID 1416605Notes

Reaction equation

HRID 1416605 reaction equation
[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][CH2:9][C@H:10]2[CH2:14][CH2:13][CH2:12][N:11]2[CH3:15])=[CH:4][CH:3]=1.[ClH:16]>>[ClH:16].[ClH:16].[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][CH2:9][C@H:10]2[CH2:14][CH2:13][CH2:12][N:11]2[CH3:15])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 54335638HCID 54335638, compound

Product 1

HCID 70200256HCID 70200256, compound

Procedure

The compound of step 36b was treated with HCl as described in Example 1b, and the title compound was isolated as a white powder. The MS and 1H NMR spectra were similar to the compound of 18c. Anal. Calc for C12H18N2OΩ2.00 HCl: C, 51.62; H, 7.22; N,10.03; Found C, 51.36; H, 7.53; N, 9.93. [α]D25=+ 6.22° (c=1, MeOH).

Sources & evidence

ORD record
ord-2ba5235dcc9841edb0983c7bc449baa2
Source dataset
uspto-grants-1999_06
Patent number
US05914328

Reaction notes

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