HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 70153691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 21309646 | HCID 21309646 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 70153691 | HCID 70153691 | — |
Reaction Steps
The 3-((1-methyl-2-(S)-pyrrolidinyl)methoxy)-5-amino-pyridine from Example 94 is dissolved in THF and reacted with acetyl chloride according to standard procedures. The product is purified by chromatography on silica gel and converted into the title compound by treatment with HCl in ether according to Example 14c.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05914328 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-8768a8e9c40642be8af6d93d011815e3 |
| Source note | uspto-grants-1999_06 |