HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → 3-((1-methyl-2-(S)-pyrrolidinyl)methoxy)-5methoxy-pyridine-N-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 3-Bromo-5-((S)-1-methyl-pyrrolidin-2-ylmethoxy)-pyridine 1-oxide | HCID 21309672 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-((1-methyl-2-(S)-pyrrolidinyl)methoxy)-5methoxy-pyridine-N-oxide | HCID 21309673 | — |
Reaction Steps
A sample of the compound from step 98a above is reacted with sodium methoxide in methanol according to standard procedures. The reaction is quenched with water, the product is extracted, then purified by chromatography on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05914328 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-1d450716c2c64c538c2ac86dc76cce6f |
| Source note | uspto-grants-1999_06 |