HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9926017, compound → 1-(2-Methylphenyl)-4-oxo-6-methyl-4,5-dihydropyrrolo[3,2-c]quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9926017 | HCID 9926017 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Diphenyl Ether | HCID 7583 | — |
| Product | 1-(2-Methylphenyl)-4-oxo-6-methyl-4,5-dihydropyrrolo[3,2-c]quinoline | HCID 15749828 | 85% |
Reaction Steps
1-(2-methylphenyl)-4-oxo-6-methyl-2,3,4,5-tetra hydropyrrolo[3,2-c]quinoline (290 mg, 1.0 mmol) was dissolved in 20 ml of diphenyl ether and 40 mg of 5% palladium/carbon was added. The reaction mixture was heated for 4 hours. The reaction mixture was cooled to the room temperature and directly purified by silica gel chromatography to obtain 245 mg of desired compound as solid in 85% of yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05914402 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-eb7118dd4a19490585f202b86d2c4d03 |
| Source note | uspto-grants-1999_06 |