Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1416679Generated: November 2, 2026

HCID 9926017, compound → 1-(2-Methylphenyl)-4-oxo-6-methyl-4,5-dihydropyrrolo[3,2-c]quinoline

https://huagongshe.com/reaction/1416679

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 9926017HCID 9926017—
CatalystPalladiumHCID 23938—
SolventDiphenyl EtherHCID 7583—
Product1-(2-Methylphenyl)-4-oxo-6-methyl-4,5-dihydropyrrolo[3,2-c]quinolineHCID 1574982885%

Reaction Steps

1-(2-methylphenyl)-4-oxo-6-methyl-2,3,4,5-tetra hydropyrrolo[3,2-c]quinoline (290 mg, 1.0 mmol) was dissolved in 20 ml of diphenyl ether and 40 mg of 5% palladium/carbon was added. The reaction mixture was heated for 4 hours. The reaction mixture was cooled to the room temperature and directly purified by silica gel chromatography to obtain 245 mg of desired compound as solid in 85% of yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05914402
Source datasetuspto-grants-1999_06
ORD IDord-eb7118dd4a19490585f202b86d2c4d03
Source noteuspto-grants-1999_06