HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1416800Generated: October 26, 2026
Glutaric Acid → Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride
https://huagongshe.com/reaction/1416800
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Glutaric Acid | HCID 743 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Edetate Sodium | HCID 6144 | — |
| Reactant | tert-Butyl hydroperoxide | HCID 6410 | — |
| Reactant | Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1) | HCID 162071 | — |
| Reactant | Ammonium Sulfate | HCID 6097028 | — |
| Reactant | Span #80 (Sorbitan monooleate) | HCID 70693544 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride | HCID 155211 | — |
Reaction Steps
General polymerization procedure. AMD, acryloxyethyltrimethylammonium chloride, ammonium sulfate, glutaric acid solution, ethylenediaminetetraacetic acid tetra sodium salt solution, isopropanol, tert-butyl hydroperoxide solution, and DI water are combined and the pH adjusted to 3.5 with sulfuric acid. Sorbitan monooleate is combined with low odor paraffin oil. The aqueous solution is slowly added to the oil solution and the combined mixture homogenized until a viscosity of 1200-1500 cps is obtained. The emulsion is sparged with nitrogen. The emulsion is heated to 40° C. The metabisulfite (MBS) solution is added at a rate to keep the reaction temperature between 40-45° C. This is maintained until the reaction conversion is at least 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05914366 |
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| Source dataset | uspto-grants-1999_06 |
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| ORD ID | ord-f9add343ffbf496bbc2e1a8ed80fdc4c |
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| Source note | uspto-grants-1999_06 |
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