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HRID1416800

反应详情

EQUATION

反应方程式

HRID 1416800 的结构方程式

REACTANTS

反应物

7
结构：O=C(O)CCCC(=O)O
HCID743

Glutaric acid

C5H8O4

结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：O=C([O-])CN(CCN(CC(=O)[O-])CC(=O)[O-])CC(=O)[O-].[Na+].[Na+].[Na+].[Na+]
HCID6144

Ethylenediaminetetraacetic acid tetrasodium salt

C10H12N2Na4O8

结构：CC(C)(C)OO
HCID6410

tert-Butyl hydroperoxide

C4H10O2

结构：C=CC(=O)OCC[N+](C)(C)C.[Cl-]
HCID162071

未命名化合物

结构：O=S(=O)([O-])[O-].[NH4+].[NH4+]
HCID6097028

Ammonium sulfate

H8N2O4S

结构：CCCCCCCC/C=C\CCCCCCCC(=O)OCC(O)[C@H]1OC[C@H](O)[C@H]1O
HCID70693544

未命名化合物

PRODUCTS

生成物

1
结构：C=CC(=O)OCC[N+](C)(C)C.C=CC(N)=O.[Cl-]
HCID155211

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：O
溶剂HCID962

Water

H2O

结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

CONDITIONS

反应条件

温度
40 °C

PROCEDURE

实验过程

General polymerization procedure. AMD, acryloxyethyltrimethylammonium chloride, ammonium sulfate, glutaric acid solution, ethylenediaminetetraacetic acid tetra sodium salt solution, isopropanol, tert-butyl hydroperoxide solution, and DI water are combined and the pH adjusted to 3.5 with sulfuric acid. Sorbitan monooleate is combined with low odor paraffin oil. The aqueous solution is slowly added to the oil solution and the combined mixture homogenized until a viscosity of 1200-1500 cps is obtained. The emulsion is sparged with nitrogen. The emulsion is heated to 40° C. The metabisulfite (MBS) solution is added at a rate to keep the reaction temperature between 40-45° C. This is maintained until the reaction conversion is at least 99%.

WORKUP

后处理

  1. customGeneral polymerization procedure
  2. additionThe aqueous solution is slowly added to the oil solution
  3. customis obtained
  4. customThe emulsion is sparged with nitrogen
  5. additionThe metabisulfite (MBS) solution is added at a rate
  6. custombetween 40-45° C
  7. temperatureThis is maintained until the reaction conversion