HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 10105410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Piperidinepropanoic acid, 1-(methoxycarbonyl)- | HCID 10262717 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10105410 | HCID 10105410 | — |
Reaction Steps
To a solution of 49.5 gm (0.23 mol) of the compound of step c), in dichloromethane, was added 0.25 mL of dimethylformamide and 21 mL of oxalyl chloride (0.25 mol). After gas evolution subsided, formation of the title compound was complete. The resulting solution was used directly into the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05916902 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-a65f946bc718464eae238f468a6c0acb |
| Source note | uspto-grants-1999_06 |