Calcium Carbonate → HCID 15389783, compound

HRID 1417058Notes

Reaction equation

HRID 1417058 reaction equation
[C:1]([C:10]1[CH:18]=[C:14]([C:15]([OH:17])=[O:16])[C:13]([OH:19])=[CH:12][CH:11]=1)(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].C(=O)([O-])[O-].[Ca+2:24]>C(O)(C)C.O>[C:1]([C:10]1[CH:18]=[C:14]([C:15]([O-:17])=[O:16])[C:13]([OH:19])=[CH:12][CH:11]=1)(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[Ca+2:24].[C:1]([C:10]1[CH:18]=[C:14]([C:15]([O-:17])=[O:16])[C:13]([OH:19])=[CH:12][CH:11]=1)(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

5

Reactant 2

HCID 10112Calcium CarbonateHCID 9838158n-Octanoyl-5-salicylic acid

Product 1

HCID 15389783HCID 15389783, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 3776IsopropanolSolvent

Procedure

39.6 g of 5-octanoylsalicylic acid (0.15 mol) in 300 ml of isopropanol and 150 ml of water were introduced into a 500 ml round-bottomed flask. 7.5 g of calcium carbonate (0.075 mol) were then added portionwise. The mixture was left stirring at room temperature for 3 hours and was then concentrated to dryness under vacuum on a rotary evaporator.

Workup

  1. waitThe mixture was left
  2. concentrationwas then concentrated to dryness under vacuum on a rotary evaporator

Sources & evidence

ORD record
ord-ae2a0ab813054b628bea66bb5277c61c
Source dataset
uspto-grants-1999_06
Patent number
US05917088

Reaction notes

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