HRID1417058

反应详情

EQUATION

反应方程式

HRID 1417058 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

39.6 g of 5-octanoylsalicylic acid (0.15 mol) in 300 ml of isopropanol and 150 ml of water were introduced into a 500 ml round-bottomed flask. 7.5 g of calcium carbonate (0.075 mol) were then added portionwise. The mixture was left stirring at room temperature for 3 hours and was then concentrated to dryness under vacuum on a rotary evaporator.

WORKUP

后处理

  1. waitThe mixture was left
  2. concentrationwas then concentrated to dryness under vacuum on a rotary evaporator